Fig. 6. (a) XRD profiles of the MoS2 powder and MoS2/Mo electrode, (b) Raman spectrum of the MoS2/Mo electrode; inset shows the electrode, (c) and (d) SEM images of the MoS2/Mo electrode, (e) SEM image of the MoS2 powder, (f) SEM image of the electrochemically treated MoS2/Mo electrode, (g) and (h) SEM images of the Au(600s)/MoS2/Mo electrode before and after the EC treatment, respectively, and (i) and (j) TEM and HRTEM images of the MoS2 powder, respectively.
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