Fig. 2. Characterization of RIE etching process of MoS2. (a) Raman spectrum and optical microscopic image of pristine MoS2 before etching. (b) Raman spectra of plasma etched MoS2 (5-2 L) for RF top-power of 150, 140, 130, 120, 110 W and RF bottom-power of 10 W, respectively. The color of each specimen is given in the inset. (c) XPS spectra of Mo 3d and S 2p for MoS2 before etching. (d) XPS spectra of Mo 3d and S 2p for MoS2 after etching. (e) Cross sectional HR-TEM image of MoS2 before etching. (f) The step height between masked and exposed regions of MoS2 before etching obtained by AFM. (g) Cross sectional HR-TEM image of MoS2 after etching. (h) The step height between masked and exposed regions of MoS2 after etching obtained by AFM. The thickness contour of 4 in. MoS2 is characterized by ellipsometry mapping with 49 points for MoS2 (i) before etching and (j) after etching.
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